By Alvin Fox, James Gilbart, Stephen L. Morgan (auth.), Alvin Fox, Stephen L. Morgan, Lennart Larsson, Göran Odham (eds.)

ISBN-10: 1489935649

ISBN-13: 9781489935649

ISBN-10: 1489935665

ISBN-13: 9781489935663

The First overseas Symposium at the Interface among Analytical Chemistry and Microbiology: functions of Chromatography and Mass Spectrometry used to be held June 1987 on the college of South Carolina, Columbia, SC, U.S.A. the aim of the "Interface" assembly was once to forge connections among analytical chemists and microbiologists which are utilizing chromatography and mass spectrometry to resolve universal difficulties. The ambitions have been admirably fulfilled. approximately 100 contributors from seven eu nations, Japan, and the USA participated in listening to twenty-three plenary talks and thirty-six submitted papers and posters. The papers and discussions displayed the breadth and intensity of present learn purposes and published destiny instructions. This ebook "Analytical Microbiology equipment: Chromatography and Mass Spectrometry" is loosely in response to a few of the shows and discussions on the assembly. every one bankruptcy describes particular technique and functions within the context of the suitable clinical history. the current publication keeps the topic of an previous publication, "Gas Chromatography/Mass Spectrometry functions in Microbiology", edited by way of G. Odham, L. Larsson, and P-A. Mardh, released through Plenum Press in 1984.

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Extra info for Analytical Microbiology Methods: Chromatography and Mass Spectrometry

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Silcox, and R. C. Good, Analysis of mycolic acid cleavage products and cellular fatty acids of Mycobacterium species by capillary gas chromatography, J. Clin. Microbiol. 23:731 (1986). K. Grob and G. Grob, Splitless injection on capillary columns, Part I. The basic technique; steroid analysis as an example, J. Chromatogr. Sci. 7:584 (1969). W. E. Harris, Some aspects of injection of large samples in gas chromatography, J. Chromatgr. Sci. 11:184 (1973). K. Grob and K. , Splitless injection and the solvent effect, HRC & CC 1:57 (1978).

Formation of negative ions by resonance capture and dissociative resonance capture in CI strongly depends on the electron affinities of sample molecules: aromatics and halogenated compounds easily form negative ions. Negative ion detection enhances selectivity and sensitivity over positive ion detection for some molecules. In analytical microbiology, negative ion chemical ionization (NICI) has been used for trace detection of halogenated derivatives of marker compounds. Selectivity is also increased since underivatized materials are not detected.

Whymann, Potentialities of coated capillary columns for gas chromatography in the petroleum industry, J. Inst. Petroleum. 45:287 (1959). K. Grob, "Classical Split and Splitless Injection in Capillary GC", Huethig, Heidelberg (1986). W. , Academic Press, New York (1980), p. 63-77. L. Larsson, E. Jantzen, and J. Johnsson, Gas chromatographic fatty acid profiles for characterization of mycobacteria: an interlaboratory methodological evaluation, Eur. J. Clin. Microbiol. 4:483 (1985). 47 18. 19. 20.

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Analytical Microbiology Methods: Chromatography and Mass Spectrometry by Alvin Fox, James Gilbart, Stephen L. Morgan (auth.), Alvin Fox, Stephen L. Morgan, Lennart Larsson, Göran Odham (eds.)


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